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I <br /> 5001 Cedar Lake Rd. <br /> ngStrom St.Louis Park,MN 55416 <br /> 952-252-0405 office <br /> nalytical 952-252-0407 fax <br /> Inc. <br /> Analysis of Bulk Samples for Asbestos Using Polarized Light Microscopy(PLM) <br /> Steve <br /> Burns Excavating <br /> 3470 Co.Rd 21 <br /> Mayer,MN 55360 <br /> Re: 426 Old Crysatl Bay <br /> Number of Samples: 54 <br /> Methods and Definitions <br /> The submitted samples were analyzed using the EPA interim Method #600/M4-82-020 (polarized light <br /> microscopy with dispersion staining). The method defines 1 an asbestos containing material as one that <br /> contains grater than 1% asbestos by weight and asbestos is defined as the fibrous forms of serpentine <br /> and certain amphiboles. While the fibrous and non-fibrous forms of minerals are discernible microscopically <br /> in hand specimens, the distinction between them is not clear on a microscopic level, especially after processing <br /> or manufacturing. Fibrous amphiboles are generally those whose mean aspect ratios (length over width) <br /> under the microscope are approximately >10; non-fibrous amphiboles are generally those whose mean <br /> aspect ratios are approximately <6. During analysis, morphology and an estimate of mean aspect ratio <br /> are used to assign a given mineral fiber population to fibrous and non-fibrous categories. That non-fibrous <br /> amphiboles are not reported as asbestos is consistent with mineralogical definitions, but does not imply that <br /> non-fibrous amphiboles are not hazardous. Airborne concentrations of them may be regulated by OSHA under <br /> certain circumstances. The type of dispersion staining used It generally phase contrast, although central stop <br /> dispersion staining may also be used. <br /> Percentage Reporting <br /> The percentage of each fiber type present was determined using volume percents estimated from stereoscopic <br /> examination, projected area percents from mounted slide examination and percents from pomparison to weight <br /> percent standards. Such estimations are suitable for most sarhpies, but do have large error ranges. Errors are <br /> estimated to be 100 relative percent uncertainty for percentage estimates under 10% ranging down to as little <br /> as 10 relative percent uncertainty for percentage estimates greater than 50%. Friable samples which have been <br /> estimated by the above methods to contain less than 10% asestos can be point counted, according to the EPA <br /> EPA Interim Methods, as required by NESHAPS. In low per ntage samples, point counting may produce false <br /> negatives or positives, due to the small number of points counted. For samples consisting of more that one <br /> apparent type of material or layer, the percentage of each fiber type of material of layer is determined and <br /> reported separately; an overall average for the sample of eachlfiber type is then calculated. The reported friability <br /> of a sample refers to that friability observed in the condition) analyzed (broken, crushed, etc.), and is not to be <br /> substituted for an on-site assessment of friability. Each Angstrom Analytical lab report relates only to the sample <br /> tested and may not, •ue to the sampling process be representative of the material sampled. <br /> March 24,2017 <br /> Kevin Hagen, • :s.-; • - &cal,Inc. <br /> Full Service Laboratory and on-site Industrial HygienelServices for the Hazardous Materials Abatement Industry <br />